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ChemicalBook CAS DataBase List Diethyl 1,3-acetonedicarboxylate

Diethyl 1,3-acetonedicarboxylate synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 95percent sulfuric acid / 1 h 20 deg C, then 3 h 50 deg C
2: H2SO4 / H2O; CHCl3 / 1 h / 35 - 40 °C

References:

Zefirov, N. S.;Sadovaya, N. K.;Kombarova, S. V. [Journal of Organic Chemistry USSR (English Translation),1988,vol. 24,p. 101 - 104][Zhurnal Organicheskoi Khimii,1988,vol. 24,# 1,p. 116 - 119]

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