1,5-dimethyl-1H-indole synthesis
- Product Name:1,5-dimethyl-1H-indole
- CAS Number:27816-53-1
- Molecular formula:C10H11N
- Molecular Weight:145.2
Yield:27816-53-1 99%
Reaction Conditions:
Stage #1: 5-methyl-1H-indolewith sodium hydride in N,N-dimethyl-formamide;mineral oil at 0 - 20; for 0.5 h;
Stage #2: methyl iodide in N,N-dimethyl-formamide;mineral oil at 0 - 20;
References:
Greulich, Tobias W.;Daniliuc, Constantin G.;Studer, Armido [Organic Letters,2015,vol. 17,# 2,p. 254 - 257] Location in patent:supporting information
10075-52-2
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