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ChemicalBook CAS DataBase List 1,5-dimethyl-1H-indole
27816-53-1

1,5-dimethyl-1H-indole synthesis

7synthesis methods
-

Yield:27816-53-1 99%

Reaction Conditions:

Stage #1: 5-methyl-1H-indolewith sodium hydride in N,N-dimethyl-formamide;mineral oil at 0 - 20; for 0.5 h;
Stage #2: methyl iodide in N,N-dimethyl-formamide;mineral oil at 0 - 20;

References:

Greulich, Tobias W.;Daniliuc, Constantin G.;Studer, Armido [Organic Letters,2015,vol. 17,# 2,p. 254 - 257] Location in patent:supporting information