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ChemicalBook CAS DataBase List 1-OXO-1,2,3,4-TETRAHYDRONAPHTHALENE-2-CARBALDEHYDE

1-OXO-1,2,3,4-TETRAHYDRONAPHTHALENE-2-CARBALDEHYDE synthesis

3synthesis methods
-

Yield:50493-08-8 88%

Reaction Conditions:

Stage #1: 3,4-dihydronaphthalene-1(2H)-onewith sodium hydride in tetrahydrofuran at 0; for 0.5 h;
Stage #2: formic acid ethyl ester in tetrahydrofuran at 25; for 3 h;

References:

Wang, Chen;Chen, Ying-Han;Wu, Hui-Chun;Wang, Cong;Liu, Yan-Kai [Organic Letters,2019,vol. 21,# 17,p. 6750 - 6755] Location in patent:supporting information

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