methyl 1,2,3,4-tetrahydro-7-methoxy-1-oxo-2-naphthalenecarboxylate synthesis
- Product Name:methyl 1,2,3,4-tetrahydro-7-methoxy-1-oxo-2-naphthalenecarboxylate
- CAS Number:120072-87-9
- Molecular formula:C13H14O4
- Molecular Weight:234.25
Yield:120072-87-9 95%
Reaction Conditions:
Stage #1: carbonic acid dimethyl esterwith sodium hydride in tetrahydrofuran;mineral oil at 65;
Stage #2: 7-Methoxy-1-tetralone in tetrahydrofuran;mineral oil at 65; for 3.16667 h;
References:
Gould, Alexandra E.;Adams, Ruth;Adhikari, Sharmila;Aertgeerts, Kathleen;Afroze, Roushan;Blackburn, Christopher;Calderwood, Emily F.;Chau, Ryan;Chouitar, Jouhara;Duffey, Matthew O.;England, Dylan B.;Farrer, Cheryl;Forsyth, Nancy;Garcia, Khristofer;Gaulin, Jeffery;Greenspan, Paul D.;Guo, Ribo;Harrison, Sean J.;Huang, Shih-Chung;Iartchouk, Natalia;Janowik, Dave;Kim, Mi-Sook;Kulkarni, Bheemashankar;Langston, Steven P.;Liu, Jane X.;Ma, Li-Ting;Menon, Saurabh;Mizutani, Hirotake;Paske, Erin;Renou, Christelle C.;Rezaei, Mansoureh;Rowland, R. Scott;Sintchak, Michael D.;Smith, Michael D.;Stroud, Stephen G.;Tregay, Ming;Tian, Yuan;Veiby, Ole P.;Vos, Tricia J.;Vyskocil, Stepan;Williams, Juliet;Xu, Tianlin;Yang, Johnny J.;Yano, Jason;Zeng, Hongbo;Zhang, Dong Mei;Zhang, Qin;Galvin, Katherine M. [Journal of Medicinal Chemistry,2011,vol. 54,# 6,p. 1836 - 1846] Location in patent:supporting information; experimental part
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