(1,1-Dimethylethyl)dimethyl[[(1R)-1-methyl-3-butyn-1-yl]oxy]silane synthesis
- Product Name:(1,1-Dimethylethyl)dimethyl[[(1R)-1-methyl-3-butyn-1-yl]oxy]silane
- CAS Number:193544-52-4
- Molecular formula:C11H22OSi
- Molecular Weight:198.38
![Butanoic acid, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-, methyl ester, (3R)-](/CAS/20200515/GIF/104524-19-8.gif)
104524-19-8
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193544-52-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: bis(2-methylpropyl)aluminium hydride / CH2Cl2 / 0.5 h / -78 °C
2.1: SO3*Py; triethylamine / CH2Cl2 / 2 h / 20 °C
2.2: PPh3 / tetrahydrofuran / 1 h / 0 °C
2.3: BuLi / tetrahydrofuran / 1 h / -78 °C
References:
Takahashi, Takashi;Kusaka, Shin-Ichi;Doi, Takayuki;Sunazuka, Toshiaki;Omura, Satoshi [Angewandte Chemie - International Edition,2003,vol. 42,# 42,p. 5230 - 5234]
![1-Butanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-, (3R)-](/CAS/20210111/GIF/109715-47-1.gif)
18162-48-6
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15448-47-2
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$50.00/1g
1066-54-2
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193544-52-4
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