1H-Benzimidazole,1-(2-methyl-2-propenyl)-(9CI) synthesis
- Product Name:1H-Benzimidazole,1-(2-methyl-2-propenyl)-(9CI)
- CAS Number:108413-23-6
- Molecular formula:C11H12N2
- Molecular Weight:172.23
Yield:108413-23-6 91%
Reaction Conditions:
Stage #1: benzoimidazolewith potassium hydroxide in dimethyl sulfoxide; for 0.75 h;Inert atmosphere;Schlenk technique;
Stage #2: 3-Chloro-2-methylpropene in dimethyl sulfoxide; for 3.5 h;Inert atmosphere;Schlenk technique;Cooling with ice;
References:
Weemers, Jarno J. M.;Sypaseuth, Fanni D.;B?uerlein, Patrick S.;Van Der Graaff, William N. P.;Filot, Ivo A. W.;Lutz, Martin;Müller, Christian [European Journal of Organic Chemistry,2014,vol. 2014,# 2,p. 350 - 362] Location in patent:supporting information
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108413-23-6
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