
2,2',4,4',5,5'-HEXACHLOROBIPHENYL synthesis
- Product Name:2,2',4,4',5,5'-HEXACHLOROBIPHENYL
- CAS Number:35065-27-1
- Molecular formula:C12H4Cl6
- Molecular Weight:360.88

108-86-1
519 suppliers
$10.00/5g

95-94-3
145 suppliers
$10.00/5g

92-52-4
415 suppliers
$9.00/5g

15862-07-4
46 suppliers
$55.00/1mg

35065-27-1
76 suppliers
$146.00/2ml
Yield:15862-07-4 52% ,92-52-4 16% ,35065-27-1 4%
Reaction Conditions:
Stage #1:bromobenzene with n-butyllithium in tetrahydrofuran;hexane for 0.333333 h;cooling;
Stage #2: with zinc(II) chloride in tetrahydrofuran;hexane at 20; for 0.333333 h;
Stage #3:1,2,4,5-tetrachlorobenzene;tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran;hexane for 24 h;Heating;Negishi coupling;
References:
Burukin;Vasil'ev;Chizhov;Zlotin [Russian Chemical Bulletin,2005,vol. 54,# 4,p. 970 - 974]

7145-82-6
63 suppliers
$9.00/5g

35065-27-1
76 suppliers
$146.00/2ml

35065-29-3
62 suppliers
$146.00/2ml

52712-04-6
28 suppliers
$155.00/1mg

35065-27-1
76 suppliers
$146.00/2ml

52663-72-6
34 suppliers
$502.89/5MG

636-30-6
233 suppliers
$31.00/25g

120-82-1
321 suppliers
$10.00/25g

35065-27-1
76 suppliers
$146.00/2ml

38380-04-0
37 suppliers
$134.00/5mg

35065-28-2
70 suppliers
$141.00/022-25mg

51908-16-8
27 suppliers
$240.00/0.5mg

636-30-6
233 suppliers
$31.00/25g

35065-27-1
76 suppliers
$146.00/2ml