2,2'-DICHLOROBIPHENYL synthesis
- Product Name:2,2'-DICHLOROBIPHENYL
- CAS Number:13029-08-8
- Molecular formula:C12H8Cl2
- Molecular Weight:223.1
1956-97-4
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13029-08-8
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Yield: 82%
Reaction Conditions:
with iron(II) chloride in tetrachloromethane at 60; for 3 h;
Steps:
General procedure for homocoupling reactions
General procedure: A mixture of arenediazonium tetrafluoroborate salt (1 mmol), FeCl2 (1 mmol) was stirred in CCl4 (2 mL) at 60 °C for 3 h. Afterward, the reaction solution was cooled to rt and filtered through a filter paper. The organic phase was evaporated under reduced pressure. The residue was purified on a SiO2 column to afford the desired product.
References:
Ding, Yiyuan;Song, Qingbao;Cheng, Kai;Qi, Chenze [Tetrahedron Letters,2012,vol. 53,# 46,p. 6269 - 6272,4]
694-80-4
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13029-08-8
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615-41-8
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3900-89-8
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148651-35-8
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$216.00/50ml
13029-08-8
59 suppliers
$75.00/100mg