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23361-67-3

2,2-Dimethyl-1-propanol formate synthesis

2synthesis methods
2987-16-8 Synthesis
3,3-dimethylbutanal

2987-16-8
214 suppliers
$5.00/1g

1070-83-3 Synthesis
3,3-Dimethylbutyric acid

1070-83-3
288 suppliers
$27.00/25mL

2,2-Dimethyl-1-propanol formate

23361-67-3
2 suppliers
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Yield:23361-67-3 63 %Chromat. ,1070-83-3 7 %Chromat.

Reaction Conditions:

with water;difluoro[4-(trifluoromethyl)phenyl]-λ3-bromane in dichloromethane at 0; for 1 h;Inert atmosphere;Baeyer-Villiger type oxidation;

References:

Ochiai, Masahito;Yoshimura, Akira;Miyamoto, Kazunori;Hayashi, Satoko;Nakanishi, Waro [Journal of the American Chemical Society,2010,vol. 132,# 27,p. 9236 - 9239] Location in patent:supporting information; experimental part