2,2-Dimethyl-1-propanol formate synthesis
2synthesis methods
- Product Name:2,2-Dimethyl-1-propanol formate
- CAS Number:23361-67-3
- Molecular formula:C6H12O2
- Molecular Weight:116.16
Yield:23361-67-3 63 %Chromat. ，1070-83-3 7 %Chromat.
Reaction Conditions:
with water;difluoro[4-(trifluoromethyl)phenyl]-λ3-bromane in dichloromethane at 0; for 1 h;Inert atmosphere;Baeyer-Villiger type oxidation;
References:
Ochiai, Masahito;Yoshimura, Akira;Miyamoto, Kazunori;Hayashi, Satoko;Nakanishi, Waro [Journal of the American Chemical Society,2010,vol. 132,# 27,p. 9236 - 9239] Location in patent:supporting information; experimental part
