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30314-63-7

2-(2-Methoxyphenyl)-1-phenylethanol synthesis

6synthesis methods
Benzenesulfonothioic acid, S-[(2-methoxyphenyl)methyl] ester

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2-(2-Methoxyphenyl)-1-phenylethanol

30314-63-7
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: iPrMgCl*LiCl / tetrahydrofuran / 1.5 h / -40 °C
1.2: 81 percent / tetrahydrofuran / 1 h / -40 - -30 °C

References:

Stoll, Armin H.;Krasovskiy, Arkady;Knochel, Paul [Angewandte Chemie - International Edition,2006,vol. 45,# 4,p. 606 - 609]