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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 2,3-DIMETHOXY-5-METHYL-BENZALDEHYDE
5701-86-0

2,3-DIMETHOXY-5-METHYL-BENZALDEHYDE synthesis

6synthesis methods
2-Methoxy-4-methylphenol

93-51-6
394 suppliers
$15.00/5g

2,3-DIMETHOXY-5-METHYL-BENZALDEHYDE

5701-86-0
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Yield:-

Steps:

Multi-step reaction with 5 steps
1.1: 95 percent / K2CO3 / acetone / 6 h / Heating
2.1: 90 percent / 24 h / 180 °C
3.1: 95 percent / KOH / methanol / 10 h / Heating
4.1: 96 percent / sodium hydroxyde / H2O / 1 h / Heating
5.1: NaHCO3; ozone / methanol; CH2Cl2 / 0.22 h / -70 °C
5.2: 80 percent / dimethyl sulfide / methanol; CH2Cl2 / 8 h / 20 °C

References:

Srikrishna;Satyanarayana [Tetrahedron,2006,vol. 62,# 12,p. 2892 - 2900]

2-methoxy-4-methyl-6-(prop-2-en-1-yl)phenol

77879-82-4
5 suppliers
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2,3-DIMETHOXY-5-METHYL-BENZALDEHYDE

5701-86-0
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References
Benzene, 2-methoxy-4-methyl-1-(2-propen-1-yloxy)-

201359-55-9
0 suppliers
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2,3-DIMETHOXY-5-METHYL-BENZALDEHYDE

5701-86-0
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References
7452-10-0 Synthesis
2-HYDROXY-3-METHOXY-5-METHYL-BENZALDEHYDE

7452-10-0
30 suppliers
$331.00/250mg

Dimethyl sulfate

77-78-1
328 suppliers
$22.00/25g

2,3-DIMETHOXY-5-METHYL-BENZALDEHYDE

5701-86-0
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References
121-33-5 Synthesis
Vanillin

121-33-5
1161 suppliers
$9.00/1g

2,3-DIMETHOXY-5-METHYL-BENZALDEHYDE

5701-86-0
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References

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