2,4-bis(4-bromophenyl)-6-phenyl-1,3,5-triazine synthesis
- Product Name:2,4-bis(4-bromophenyl)-6-phenyl-1,3,5-triazine
- CAS Number:137726-53-5
- Molecular formula:C21H13Br2N3
- Molecular Weight:467.16
55368-42-8
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Yield:137726-53-5 85%
Reaction Conditions:
with potassium carbonate;sulfur in dimethyl sulfoxide at 120; for 12 h;
Steps:
3
Preparation method: adding 1.0 mmol of 4-bromobenzylhydrazine hydrochloride, 1.0 mmol of benzyl chloride, 0.75 mmol of sulfur powder, 1.5 mmol of K2CO3, and then adding 2 mL of dimethyl sulfoxide in a 25 mL pressure tube, and stirring at 120 ° C for 12 hours. The TLC plate detected complete reaction and product formation.The reaction solution was cooled, extracted, dried, evaporated under reduced pressure, and then filtered to afford white solid.
References:
CN110054593,2019,A Location in patent:Paragraph 0034-0039
16796-52-4
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55368-42-8
131 suppliers
$11.00/1g
100-52-7
971 suppliers
$20.37/250g
137726-53-5
14 suppliers
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623-00-7
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98-88-4
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