2,4-DINITROBENZYL CHLORIDE synthesis
- Product Name:2,4-DINITROBENZYL CHLORIDE
- CAS Number:610-57-1
- Molecular formula:C7H5ClN2O4
- Molecular Weight:216.58
99-65-0
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75-09-2
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610-57-1
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$39.70/1g
Yield: 83%
Reaction Conditions:
Stage #1:dichloromethane with n-butyllithium in tetrahydrofuran;hexane at -100; for 0.333333 h;Inert atmosphere;
Stage #2:meta-dinitrobenzene in tetrahydrofuran;hexane at -100; for 0.00833333 h;Inert atmosphere;
Stage #3: with trifluorormethanesulfonic acid in tetrahydrofuran;hexane;water at -100 - 20;Inert atmosphere;
References:
Khutorianskyi, Viktor V.;Klepetářová, Blanka;Beier [Organic Letters,2019,vol. 21,# 14,p. 5443 - 5446] Location in patent:supporting information
100-14-1
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610-57-1
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612-23-7
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$60.00/500mg
610-57-1
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100-44-7
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$13.50/250G
610-57-1
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$39.70/1g