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ChemicalBook CAS DataBase List 2-BUTANOL

2-BUTANOL synthesis

15synthesis methods
-

Yield:15892-23-6 100%

Reaction Conditions:

with hydrogen in water at 100; under 11251.1 Torr; for 0.5 h;Concentration;

Steps:

6 Example: 6

To 1 g of 2-butanone in 40 ml of H20, HRO/Na-β catalyst (50 mg) was added in a reactorvessel. The reactor vessel was then heated at 100 °C for 30 mm under H2 pressure (15 bar).After completion of the reaction, the catalyst was separated by using centrifuge and theobtained clear product mixture was analyzed by GC-MS. The reaction gave 100% conversion of 2-butanone with 100% yield of 2-butanol.

References:

WO2017/60922,2017,A1 Location in patent:Page/Page column 13; 19, 20

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