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ChemicalBook CAS DataBase List 2-Chloro-N,N-diisopropylbenzaMide, 97%
70657-63-5

2-Chloro-N,N-diisopropylbenzaMide, 97% synthesis

4synthesis methods
-

Yield:70657-63-5 92%

Reaction Conditions:

Stage #1: N,N-diisopropyl benzamidewith (2,2,6,6-tetramethylpiperidido)2Ag(CN)Li2 at 0; for 0.5 h;
Stage #2: with N-chlorophthalimide at 20; for 1 h;chemoselective reaction;Reagent/catalyst;

References:

Tezuka, Noriyuki;Hirano, Keiichi;Peel, Andrew J.;Wheatley, Andrew E. H.;Miyamoto, Kazunori;Uchiyama, Masanobu [Chemical Science,2020,vol. 11,# 7,p. 1855 - 1861]