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(2-CHLORO-PYRIDIN-4-YL)-DIMETHYL-AMINE synthesis

9synthesis methods
1122-58-3 Synthesis
4-Dimethylaminopyridine

1122-58-3
1012 suppliers
$6.00/1g

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Yield:59047-70-0 90%

Reaction Conditions:

Stage #1: dmapwith n-butyllithium;2-(N,N-dimethylamino)ethanol in hexane at 0; for 1 h;
Stage #2: with hexachloroethane in hexane at -78 - 0; for 1.5 h;Further stages.;

References:

Cuperly, David;Gros, Philippe;Fort, Yves [Journal of Organic Chemistry,2002,vol. 67,# 1,p. 238 - 241]

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