2-HYDROXYACETAMIDE synthesis
- Product Name:2-HYDROXYACETAMIDE
- CAS Number:598-42-5
- Molecular formula:C2H5NO2
- Molecular Weight:75.07
96-35-5
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$5.00/5g
598-42-5
79 suppliers
$61.00/1g
Yield:598-42-5 94%
Reaction Conditions:
with urea at 160; for 3 h;Reagent/catalyst;Temperature;
Steps:
1-4; 1-3; 5 Preparation of ethanolamide:
Add 450g of methyl glycolate, 100g of urea and 15g of the obtained solid-liquid composite catalyst (5g of platinum-based solid catalyst-10g of tetraethyl titanate liquid) into a three-necked flask, raise the temperature to 160°C, react for 3 hours, and proceed with stirring ,As shown in Figure 3.After the reaction was completed and cooled, filtered and analyzed, the yield was calculated, and the yield of ethanolamide was 94%.
References:
CN112608244,2021,A Location in patent:Paragraph 0047; 0050-0052; 0055-0057; 0059-0060; 0062-0063
79-14-1
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598-42-5
79 suppliers
$61.00/1g
623-50-7
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$5.00/1g
598-42-5
79 suppliers
$61.00/1g
67-56-1
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$9.00/25ml
598-42-5
79 suppliers
$61.00/1g
108-13-4
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598-41-4
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$185.00/1kg