4-AMino-N-ethylphthaliMide synthesis
- Product Name:4-AMino-N-ethylphthaliMide
- CAS Number:55080-55-2
- Molecular formula:C10H10N2O2
- Molecular Weight:190.2
55080-56-3
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55080-55-2
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Yield:55080-55-2 92%
Reaction Conditions:
with hydrogenchloride;tin(II) chloride dihdyrate in water; for 2.5 h;
Steps:
1.3 2.5.1.3. 4-Amino-N- ethylphthalimide (MB2).
N- Ethyl-4-nitrophthalimide (22 g) was stirred into a solution of stannouschloride dihydrate (100 g) in hydrochloric acid (37%, 100 ml) andwater (100 ml). After 2.5 h, the precipitate was collected bydrowning onto ice. Filtered and washed with cold water until freefrom acid. The product was purified by recrystallisation fromtoluene. Yield: 92%.
References:
Zhan, Yizhen;Zhao, Xue;Wang, Wei [Dyes and Pigments,2017,vol. 146,p. 240 - 250]
89-40-7
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$5.00/5g
55080-55-2
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85-41-6
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$9.00/1g
55080-55-2
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