4-BUTOXYBENZOHYDRAZIDE synthesis
- Product Name:4-BUTOXYBENZOHYDRAZIDE
- CAS Number:64328-61-6
- Molecular formula:C11H16N2O2
- Molecular Weight:208.26
4906-25-6
46 suppliers
$32.39/10g
64328-61-6
26 suppliers
inquiry
Yield:64328-61-6 91%
Reaction Conditions:
with hydrazine hydrate in methanol at 70;
Steps:
1
33.9 g (163 mmol) of methyl 4-butoxybenzoate, 150 ml of hydrazine hydrate (80%) and 500 ml of methanol were added to a 1000 ml three-necked flask, and heated to reflux at 70 °C. After the reaction was completed, the reaction solution was spin-dried to obtain a white solid. The white solid was washed three times with water and filtered to finally obtain 30 g of 4-butoxybenzoylhydrazide (yield: 91%)
References:
CN110272364,2019,A Location in patent:Paragraph 0044; 0046
1498-96-0
111 suppliers
$9.00/1g
64328-61-6
26 suppliers
inquiry
5365-43-5
2 suppliers
inquiry
64328-61-6
26 suppliers
inquiry
99-76-3
747 suppliers
$5.00/25g
64328-61-6
26 suppliers
inquiry
120-47-8
668 suppliers
$5.00/100mg
64328-61-6
26 suppliers
inquiry