ChemicalBook CAS DataBase List 4-CHLORO-2-ANISIDINE HYDROCHLORIDE

4-CHLORO-2-ANISIDINE HYDROCHLORIDE synthesis

11synthesis methods

Product Name:4-CHLORO-2-ANISIDINE HYDROCHLORIDE
CAS Number:93-50-5
Molecular formula:C7H8ClNO
Molecular Weight:157.6

67-56-1 Synthesis

67-56-1
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$7.29/5ml-f

100-00-5
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$14.00/25g

93-50-5
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$21.00/250mg

Yield: 28%

Reaction Conditions:

with fac-tris(2-phenylpyridinato-N,C₂')iridium(III);methanesulfonic acid;triphenylphosphine in acetonitrile at 55; for 24 h;Irradiation;Inert atmosphere;

Steps:

8 Examples 1-16
General procedure: Step 1: Add the nitro compound (see Table 1 for specific substances) and methanol into the reaction vessel, and add the reducing agent (with(See Table 1 for specific substances), photocatalyst (see Table 1 for specific substances), water (see Table 1 for specific materials), organic acids (see Table 1 for specific substances)1) Add the organic solvent (see Table 1 for specific substances) into the reaction vessel.

References:

CN112812027, 2021, A Location in patent:Paragraph 0027; 0030-0032; 0041-0042