ChemicalBook CAS DataBase List (4-HYDROXYPHENYL)(M-TOLYL)METHANONE

(4-HYDROXYPHENYL)(M-TOLYL)METHANONE synthesis

4synthesis methods

Product Name:(4-HYDROXYPHENYL)(M-TOLYL)METHANONE
CAS Number:71372-37-7
Molecular formula:C14H12O2
Molecular Weight:212.24

Preparation by Fries rearrangement of phenyl m-toluate in the presence of aluminium chloride in refluxing carbon disulfide for 2 h, then elimination of the solvent and heating at 150° for 3 h (major product).

53039-63-7
11 suppliers
$294.00/1g

71372-37-7
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Yield:71372-37-7 56%

Reaction Conditions:

with sodium thiomethoxide in N,N-dimethyl-formamide; for 5 h;Heating;

References:

Kubo, Kazuo;Ohyama, Shin-Ichi;Shimizu, Toshiyuki;Takami, Atsuya;Murooka, Hideko;Nishitoba, Tsuyoshi;Kato, Shinichiro;Yagi, Mikio;Kobayashi, Yoshiko;Iinuma, Noriko;Isoe, Toshiyuki;Nakamura, Kazuhide;Iijima, Hiroshi;Osawa, Tatsushi;Izawa, Toshio [Bioorganic and Medicinal Chemistry,2003,vol. 11,# 23,p. 5117 - 5133]

100-66-3 Synthesis

100-66-3
509 suppliers
$10.00/5G

71372-37-7
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References

1711-06-4 Synthesis

1711-06-4
302 suppliers
$6.00/25g

71372-37-7
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References

99-04-7 Synthesis

99-04-7
429 suppliers
$8.00/100g

71372-37-7
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References

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