4-Iodobenzoyl chloride synthesis
- Product Name:4-Iodobenzoyl chloride
- CAS Number:1711-02-0
- Molecular formula:C7H4ClIO
- Molecular Weight:266.46
619-58-9
443 suppliers
$8.00/5g
1711-02-0
163 suppliers
$10.00/1g
Yield:1711-02-0 100%
Steps:
1 (1)
(1) Synthesis of p-iodobenzoyl Chloride An eggplant type flask was charged with 46.2 g of p-iodobenzoic acid and 1,000 mL (milliliters) of thionyl chloride, and the p-iodobenzoic acid was dissolved. Then, the mixture was refluxed under heat for 3 hours. Thionyl chloride was distilled off under reduced pressure, to give 49.6 g of an end compound (crude product yield 100%).
References:
Mitsubishi Gas Chemical Co., Inc. US2003/102459, 2003, A1
79-37-8
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$17.67/10gm:
619-58-9
443 suppliers
$8.00/5g
1711-02-0
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$10.00/1g
624-38-4
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$6.00/5g
122-04-3
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636-98-6
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$17.00/5g
1711-02-0
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$10.00/1g
10486-61-0
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100-20-9
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41507-35-1
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$45.00/100mg
1711-02-0
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$10.00/1g
79-37-8
482 suppliers
$17.67/10gm:
591-50-4
504 suppliers
$10.00/1g
1711-02-0
163 suppliers
$10.00/1g