(4-METHOXY-BENZYL)-TRIMETHYL-SILANE synthesis
- Product Name:(4-METHOXY-BENZYL)-TRIMETHYL-SILANE
- CAS Number:17988-20-4
- Molecular formula:C11H18OSi
- Molecular Weight:194.35
104-92-7
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1822-00-0
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$108.00/50ml
17988-20-4
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Yield:17988-20-4 98%
Reaction Conditions:
Stage #1: 1-bromo-4-methoxy-benzenewith bis(tri-t-butylphosphine)palladium(0);oxygen in toluene at 20; for 0.0166667 h;Schlenk technique;
Stage #2: trimethylsilylmethyllithium in toluene at 20; for 0.0333333 h;Schlenk technique;
References:
Heijnen, Dorus;Tosi, Filippo;Vila, Carlos;Stuart, Marc C. A.;Elsinga, Philip H.;Szymanski, Wiktor;Feringa, Ben L. [Angewandte Chemie - International Edition,2017,vol. 56,# 12,p. 3354 - 3359][Angew. Chem.,2017,vol. 129,# 12,p. 3402 - 3407,6] Location in patent:supporting information
623-12-1
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13170-43-9
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$45.00/1mL
17988-20-4
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1450-14-2
287 suppliers
$29.12/10ML
104-47-2
462 suppliers
$6.00/10g
17988-20-4
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623-12-1
297 suppliers
$10.00/25g
1822-00-0
118 suppliers
$108.00/50ml
17988-20-4
11 suppliers
inquiry