4-Nitro-2-(trifluoromethyl)benzoyl chloride synthesis
- Product Name:4-Nitro-2-(trifluoromethyl)benzoyl chloride
- CAS Number:98187-15-6
- Molecular formula:C8H3ClF3NO3
- Molecular Weight:253.56
392-83-6
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: sulfuric acid; nitric acid / 20 °C
2.1: methyl iodide; magnesium; iodine / tetrahydrofuran / 3 h / 50 °C / Inert atmosphere
2.2: 2 h / Inert atmosphere
3.1: thionyl chloride / 2 h / Reflux
References:
Shenzhen Daoerdun Electronic Materials Co., Ltd.;Wang Shenglin;Li Houming;Wang Jianxin CN112225676, 2021, A
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367-67-9
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