
5-PHENYL-N-VALERIC ACID METHYL ESTER synthesis
- Product Name:5-PHENYL-N-VALERIC ACID METHYL ESTER
- CAS Number:20620-59-1
- Molecular formula:C12H16O2
- Molecular Weight:192.25

2270-20-4
183 suppliers
$11.00/1g

18107-18-1
214 suppliers
$33.00/5g

20620-59-1
68 suppliers
$45.00/50mg
Yield: 66 %Chromat.
Reaction Conditions:
in methanol;diethyl ether at 0 - 20;
Steps:
4.3. General procedure for the oxidation of the long chainalcohol 3a-3h
General procedure: To the solution of the mixture in diethyl ether (5 mL) andmethanol (4 mL) in ice bath, a solution of trimethysilyldiazomethanein diethyl ether (2 mL, 2 M, 4 mmol) was added dropwisewhile stirring, and stirring for 2 h, then ice bath was removed andstirring overnight. Upon removal of residual solvents and trimethylsilylspecies, the product was obtained and the product wasdetected by GCeMS. The original spectra of GCeMS were given inthe Supplementary data.
References:
Yu, Dong-Fang;Xing, Ping;Jiang, Biao [Tetrahedron,2015,vol. 71,# 25,p. 4269 - 4273]

67-56-1
776 suppliers
$7.29/5ml-f

2270-20-4
183 suppliers
$11.00/1g

20620-59-1
68 suppliers
$45.00/50mg

17376-04-4
88 suppliers
$24.03/1gm:

292638-85-8
4 suppliers
inquiry

20620-59-1
68 suppliers
$45.00/50mg

867-13-0
484 suppliers
$10.00/1g

103-26-4
566 suppliers
$6.00/25g

20620-59-1
68 suppliers
$45.00/50mg

103-63-9
513 suppliers
$9.00/10g

292638-85-8
4 suppliers
inquiry

20620-59-1
68 suppliers
$45.00/50mg