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ChemicalBook CAS DataBase List tert-butyl ((1r,4r)-4-Morpholinocyclohexyl)carbaMate
558442-96-9

tert-butyl ((1r,4r)-4-Morpholinocyclohexyl)carbaMate synthesis

5synthesis methods
-

Yield:558442-96-9 100 mg

Reaction Conditions:

with potassium carbonate in N,N-dimethyl-formamide at 100;

Steps:

44

S-139 (200 mg) was converted to S-140 using 3-oxa-l ,5-dichloropentane in the presence of K2CO3 and heating the reaction at 100 °C in DMF overnight. After purification, 100 mg of S-140 was obtained.

References:

WO2019/136244,2019,A1 Location in patent:Page/Page column 154

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