Bis(trimethylsilylcyclopentadienyl)zirconium dichloride synthesis
- Product Name:Bis(trimethylsilylcyclopentadienyl)zirconium dichloride
- CAS Number:60938-59-2
- Molecular formula:C16H26Cl2Si2Zr
- Molecular Weight:436.68
29943-00-8
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29942-99-2
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10026-11-6
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60938-59-2
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Yield:60938-59-2 75%
Reaction Conditions:
with n-butyllithium in diethyl ether;hexane;byproducts: n-butane, LiCl; addn. of soln. of n-butyllithium in hexane to soln. of isomeric mixture of cyclopentadiene derivative at -78 °C, addn. of ZrCl4 at -78 °C, stirred over night at room temp.; suspn. filtered of Na2SO4, evapn. in vac., washed with n-pentane, dried in vac;
References:
Licht, Andrea I.;Alt, Helmut G. [Journal of Organometallic Chemistry,2003,vol. 684,# 1-2,p. 91 - 104]
3559-74-8
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$42.00/1g
10026-11-6
225 suppliers
$24.80/50g
60938-59-2
14 suppliers
inquiry
![Stannane, dimethylbis[1-(trimethylsilyl)-2,4-cyclopentadien-1-yl]-](/CAS/20210305/GIF/945212-07-7.gif)