Dimethyl 2,6-dimethyl-4-phenylpyridine-3,5-dicarboxylate synthesis
- Product Name:Dimethyl 2,6-dimethyl-4-phenylpyridine-3,5-dicarboxylate
- CAS Number:77234-00-5
- Molecular formula:C17H17NO4
- Molecular Weight:299.32
Yield: 80%
Reaction Conditions:
with graphite oxide in water for 5 h;Reflux;Hantzsch Dihydropyridine Synthesis;
Steps:
Typical procedure for the synthesis of pyridines usinggraphite oxide (GO)
General procedure: A mixture of aldehyde 1a-1j (1 mmol), methyl 3-aminocrotonate(5 mmol), and amount of GO (as indicated inTable 2) was stirred in reflux of solvent under ambient airfor indicated time in Table 2. After completion of thereaction, the residue was dissolved in CH2Cl2 and filteredthrough a sintered funnel. The filtrate was evaporated andpurified by recrystallization from EtOH
References:
Mirza-Aghayan, Maryam;Asadi, Fatemeh;Boukherroub, Rabah [Monatshefte fur Chemie,2014,vol. 145,# 12,p. 1919 - 1924]
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)