8-AMINO-1,2,3,4-TETRAHYDROQUINOLINE synthesis
- Product Name:8-AMINO-1,2,3,4-TETRAHYDROQUINOLINE
- CAS Number:54012-92-9
- Molecular formula:C9H12N2
- Molecular Weight:148.21
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / chloroform / 4 h / Reflux
2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver(I) triflimide; silver(I) acetate / methanol / 12 h / 50 °C / 760.05 Torr
3: ammonium formate; 5%-palladium/activated carbon / methanol / 12 h / 25 °C / 760.05 Torr
References:
Gwon, Donghyeon;Hwang, Heejun;Kim, Hye Kyung;Marder, Seth R.;Chang, Sukbok [Chemistry - A European Journal,2015,vol. 21,# 48,p. 17200 - 17204]
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