9-N-OCTYLCARBAZOLE synthesis

5synthesis methods

Product Name:9-N-OCTYLCARBAZOLE
CAS Number:4041-19-4
Molecular formula:C20H25N
Molecular Weight:279.42

629-27-6 Synthesis

629-27-6
145 suppliers
$5.00/5g

86-74-8 Synthesis

86-74-8
318 suppliers
$10.00/5g

4041-19-4
10 suppliers
$1797.18/25G

Yield:-

Reaction Conditions:

with sodium hydroxide in acetone; for 10 h;Reflux;Inert atmosphere;

Steps:

5

Synthesis Example 5; Compound A-5 was synthesized by the method illustrated in Scheme 5.; To 200 ml of acetone were added 6.33 g of compound (5-a) (produced by Tokyo Chemical Industry Co., Ltd.), 10 g of 1-iodooctane (produced by Wako Pure Chemical Industries, Ltd.) and 2.27 g of NaOH, and the resulting mixture was refluxed for 10 hours under heating under a nitrogen atmosphere. To the resulting solution were added water and hexane. Then, an organic layer was fractionated, washed with water, and then dried with magnesium sulfate. The resulting solution was purified by column chromatography (filler: silica gel, eluent: dichloromethane/hexane) to obtain 4.82 g of compound (5-b).

References:

EP2266982,2010,A1 Location in patent:Page/Page column 31-32

111-83-1 Synthesis