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ChemicalBook CAS DataBase List 9-(TRIMETHYLSILYL)FLUORENE

9-(TRIMETHYLSILYL)FLUORENE synthesis

8synthesis methods
-

Yield:7385-10-6 98%

Reaction Conditions:

Stage #1: 9H-fluorenewith n-butyllithium in diethyl ether;hexane at -78;
Stage #2: chloro-trimethyl-silane in diethyl ether;hexane at -78;

References:

Silaghi-Dumitrescu, Ioan;Cretiu, Gabriela;Silaghi-Dumitrescu, Luminita;Haiduc, Ionel;Toscano, Alfredo;Cea-Olivares, Raymundo [Revue Roumaine de Chimie,2001,vol. 46,# 4,p. 289 - 295]

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