Bathophenanthroline synthesis
- Product Name:Bathophenanthroline
- CAS Number:1662-01-7
- Molecular formula:C24H16N2
- Molecular Weight:332.4
Yield:1662-01-7 76.4%
Reaction Conditions:
with hydrogenchloride;hydrogen iodide in water at 100; for 0.333333 h;Reagent/catalyst;Temperature;
Steps:
1; 2; 3; 4; 5 Embodiment 4:
A solution of 3-chloropropiophenone (concentration 0.4 mol/L) and o-phenylenediamine (concentration 0.2 mol/L) mixed acid (30% hydrochloric acid concentration, 20% hydroiodic acid concentration) was pumped into the microchannel reaction at a rate of 30 ml/min. The reactor (with a 5 mm umbrella quartz reactor) was kept at a constant temperature of 100 ° C for 20 min, and the effluent was cooled. After filtration, the filter cake was rinsed twice with ammonia, and dried to give a yellow solid product, yield 76.4%.
References:
CN109456325,2019,A Location in patent:Paragraph 0025; 0026; 0027; 0028-0034
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