Benzoic acid, 2-formyl-5-nitro-, methyl ester synthesis
- Product Name:Benzoic acid, 2-formyl-5-nitro-, methyl ester
- CAS Number:142314-69-0
- Molecular formula:C9H7NO5
- Molecular Weight:209.16
Yield:142314-69-0 94%
Reaction Conditions:
Stage #1: 3-hydroxy-6-nitro-1-(3H)isobenzofuranonewith 1,8-diazabicyclo[5.4.0]undec-7-ene in acetone; for 0.166667 h;
Stage #2: methyl iodide in acetone at 20; for 4 h;
References:
Mal, Dipakranjan;Jana, Amit;Ray, Sutapa;Bhattacharya, Sourav;Patra, Asit;De, Saroj R. [Synthetic Communications,2008,vol. 38,# 22,p. 3937 - 3946] Location in patent:experimental part
![Benzoic acid, 2-[bis(acetyloxy)methyl]-5-nitro-, methyl ester](/CAS/20210305/GIF/198821-81-7.gif)
198821-81-7
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