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ChemicalBook CAS DataBase List BOC-THIONOLEU-1-(6-NITRO)BENZOTRIAZOLIDE
214750-70-6

BOC-THIONOLEU-1-(6-NITRO)BENZOTRIAZOLIDE synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 24.5 h / -10 - 20 °C / Inert atmosphere
2: tetraphosphorus decasulfide; sodium carbonate / tetrahydrofuran / 23 h / 20 °C / Inert atmosphere
3: acetic acid; sodium nitrite / water / 30 min / 0 - 20 °C

References:

WO2022/244821,2022,A1

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