ethyl 2-(2,4-difluorophenyl)acetate synthesis
- Product Name:ethyl 2-(2,4-difluorophenyl)acetate
- CAS Number:129409-54-7
- Molecular formula:C10H10F2O2
- Molecular Weight:200.18
64-17-5
824 suppliers
$10.00/50g
81228-09-3
274 suppliers
$12.00/2g
129409-54-7
26 suppliers
$85.00/1G
Yield:129409-54-7 95.5%
Reaction Conditions:
with sulfuric acid at 20; for 48 h;
Steps:
19
Concentrated sulfuric acid (3 mL) was added slowly to a stirred solution of 2,4 di- fluorophenylacetic acid a (10.0 g, 58.1 mmol) in EtOH (100 mL), stirred at RT for 2 d. It was concentrated, diluted with EtOAc (200 mL), washed with 10% K2CO3 until the washes EPO
References:
WO2006/69063,2006,A1 Location in patent:Page/Page column 87-88