ethyl 2,2-dimethylpent-4-enoate synthesis
- Product Name:ethyl 2,2-dimethylpent-4-enoate
- CAS Number:86549-27-1
- Molecular formula:C9H16O2
- Molecular Weight:156.22
Yield:86549-27-1 93%
Reaction Conditions:
Stage #1: Ethyl isobutyratewith n-butyllithium;diisopropylamine in tetrahydrofuran;hexane at -78; for 1 h;
Stage #2: allyl bromide in tetrahydrofuran;hexane at -78; for 1 h;
References:
Baader, Sabrina;Ohlmann, Dominik M.;Goossen, Lukas J. [Chemistry - A European Journal,2013,vol. 19,# 30,p. 9807 - 9810] Location in patent:supporting information
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