ethyl 2-(allyl(tert-butoxycarbonyl)aMino)acetate synthesis
- Product Name:ethyl 2-(allyl(tert-butoxycarbonyl)aMino)acetate
- CAS Number:251948-87-5
- Molecular formula:C12H21NO4
- Molecular Weight:243.3
Yield:251948-87-5 61%
Reaction Conditions:
Stage #1: ethyl 2-(tert-butoxycarbonylamino)acetatewith P-tris(dimethylamino)-C-dimethylphosphonium ylide in tetrahydrofuran at -78; for 1 h;Substitution;
Stage #2: allyl bromide in tetrahydrofuran; for 48 h;Heating;Alkylation;
References:
Palacios, Francisco;Aparicio, Domitila;De Los Santos, Jesús M.;Baceiredo, Antoine;Bertrand, Guy [Tetrahedron,2000,vol. 56,# 4,p. 663 - 669]
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