ETHYL 2-AMINO-5-METHYLBENZOATE synthesis
- Product Name:ETHYL 2-AMINO-5-METHYLBENZOATE
- CAS Number:58677-05-7
- Molecular formula:C10H13NO2
- Molecular Weight:179.22
2941-78-8
58677-05-7
General procedure for the synthesis of ethyl 2-amino-5-methylbenzoate (compound of formula VII) from 2-amino-5-methylbenzoic acid: following the method reported by SP Acharya and JB Hynes in Journal of Heterocyclic Chemistry (1975,12,1283), the 2-amino-5-methyl benzoic acid was reacted with ethanol catalyzed by HCl gas to obtain the target product. Yield: 80%. The product was a white solid with mass spectrum (ISP) m/z 178 (M-H).
54064-40-3
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58677-05-7
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Yield:58677-05-7 98%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in ethanol; under 760.051 Torr; for 168 h;Darkness;
References:
Bhuiyan, M. Delower H.;Zhu, Kai-Xian;Jensen, Paul;Try, Andrew C. [European Journal of Organic Chemistry,2010,# 24,p. 4662 - 4670] Location in patent:supporting information; experimental part
2941-78-8
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58677-05-7
74 suppliers
$35.00/1g
2941-78-8
486 suppliers
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58677-05-7
74 suppliers
$35.00/1g