ethyl 4-(ethylamino)benzoate synthesis
- Product Name:ethyl 4-(ethylamino)benzoate
- CAS Number:42265-58-7
- Molecular formula:C11H15NO2
- Molecular Weight:193.24
Yield:42265-58-7 98.5%
Reaction Conditions:
with hydrogen in ethanol at 170; under 15001.5 Torr; for 9 h;
Steps:
2.5 Catalytic reactions and product analysis
The nitroarenes (0.81mmol), alcohols and the as-synthesized catalysts were placed in reactor (100mL). Before hydrogenation-alkylation tandem experiments, the reactor was purged with N2 and H2 to remove the air and N2 for three times, respectively. The reaction mixture were isolated by the magnet, and the isolated NiCo/MgO-C catalyst was washed with ethanol and dried before reused for recyclability measurement. The conversions and yields of reactions of hydrogenation-alkylation tandem reaction were analyzed by using GC-MS.
References:
Li, Weizuo;Wang, Jing;He, Dafang;He, Guangyu;Chen, Haiqun [Molecular catalysis,2022,vol. 529,art. no. 112520]
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