Fumaric acid synthesis
- Product Name:Fumaric acid
- CAS Number:110-17-8
- Molecular formula:C4H4O4
- Molecular Weight:116.07
110-16-7
685 suppliers
$10.00/5g
110-17-8
1004 suppliers
$9.00/5g
Yield:110-17-8 99.5%
Reaction Conditions:
with maleic anhydride in lithium hydroxide monohydrate at 190; for 6 h;Inert atmosphere;Autoclave;Green chemistry;Reagent/catalyst;
Steps:
4
Saturated malic acid in the mother liquid and the water suction filtrate lossy process, the need to fill the filtrate in Example 3 plus a certain amount of the mass of 306g at a concentration of 50%, together with 300g of maleic anhydride was added to a 1000ml autoclave in with N2 Air autoclave was replaced three times at 190 degree, speed of 300 rev / min under conditions of reaction 6h, after the reaction to adjust speed of 100 rev / min to cool to room temperature. Remove the liquid crystalline fumaric acid, fumaric acid filtration to give crystals, placed in 80 oven bake 4h. Finally get fumaric 353.3g, a yield of 99.5%.
References:
CN103601636,2016,B Location in patent:Paragraph 0034; 0035
108-31-6
823 suppliers
$13.47/50g
110-17-8
1004 suppliers
$9.00/5g
98-01-1
464 suppliers
$22.00/25g
88-14-2
481 suppliers
$5.00/10g
110-15-6
901 suppliers
$5.00/10g
110-16-7
685 suppliers
$10.00/5g
110-17-8
1004 suppliers
$9.00/5g
617-48-1
285 suppliers
$16.60/100G
110-17-8
1004 suppliers
$9.00/5g
201230-82-2
1 suppliers
inquiry
74-86-2
71 suppliers
inquiry
110-15-6
901 suppliers
$5.00/10g
110-17-8
1004 suppliers
$9.00/5g