Glycidyl Linoleate synthesis
- Product Name:Glycidyl Linoleate
- CAS Number:24305-63-3
- Molecular formula:C21H36O3
- Molecular Weight:336.51
60-33-3
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$9.00/5g
106-89-8
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24305-63-3
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$155.00/10mg
Yield:24305-63-3 309.8 g
Reaction Conditions:
Stage #1: (Z,Z)-9,12-octadecadienoic acid;(±)-epichlorohydrinwith benzyl-triethyl-ammonium chloride at 80; for 1.5 h;
Stage #2: with sodium hydroxide at 40; for 4 h;
Steps:
4 Example 4
Add 280.4 g (1 mol) of linoleic acid, 323.8 g (3.5 mol) of epichlorohydrin, and 7.1 g of benzyltriethylammonium chloride to a tetrahedron equipped with a mechanical stirrer with a mechanical seal, a reflux condenser and a thermometer. In the flask, the temperature of the ring-opening esterification reaction was controlled to be 80°C, and the reaction was kept for 1.5 h to obtain 611.3 g of the ring-opening esterification reaction mixture with an acid value of 0.3509 mg KOH/g.
References:
CN113896636,2022,A Location in patent:Paragraph 0078-0079
7459-33-8
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$203.00/1g
556-52-5
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$17.67/1gm:
24305-63-3
14 suppliers
$155.00/10mg
60-33-3
547 suppliers
$9.00/5g
556-52-5
244 suppliers
$17.67/1gm:
24305-63-3
14 suppliers
$155.00/10mg
60-33-3
547 suppliers
$9.00/5g
24305-63-3
14 suppliers
$155.00/10mg