ChemicalBook CAS DataBase List Iprobenfos

Iprobenfos synthesis

11synthesis methods

Product Name:Iprobenfos
CAS Number:26087-47-8
Molecular formula:C13H21O3PS
Molecular Weight:288.34

1809-20-7 Synthesis

1809-20-7
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100-53-8
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26087-47-8
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$46.70/100mg

Yield:26087-47-8 87%

Reaction Conditions:

with oxygen;caesium carbonate in acetonitrile at 80; under 760.051 Torr; for 12 h;

Steps:

35 Example 35 Synthesis of different rice blast
A 25 mL reaction tube was charged, 41.0 mg of cesium carbonate was added, 41.6 mg of diisopropyl phosphite, benzyl mercaptan46.6 mg, acetonitrile 1 mL, stirred at 80 ° C for 12 hours, and the gas atmosphere was a standard atmospheric pressure of oxygen. After the end of the reaction, the residue was purified by column chromatography to yield 62.7 mg of rice blast.

References:

Peking University;Jiao Ning;Zhang Yiqun;Song Song CN106905361, 2017, A Location in patent:Paragraph 0235; 0236; 0237; 0238

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1809-20-7 Synthesis

1809-20-7
170 suppliers
$8.00/10g