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ChemicalBook CAS DataBase List ISOXAFLUTOLE

ISOXAFLUTOLE synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran / 3.6 h / 52 °C
1.2: 19.5 h / 22 °C
2.1: acetic anhydride / 3.8 h / Reflux
2.2: 1.82 h / 20 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16.2 h / -13 - 20 °C

References:

Wuxi Jiabao Pharmaceutical Co., Ltd.;Wang Xiangrong CN107162995, 2017, A

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