N-(3-nitrophenyl)methanesulfonamide synthesis
3synthesis methods
- Product Name:N-(3-nitrophenyl)methanesulfonamide
- CAS Number:63228-62-6
- Molecular formula:C7H8N2O4S
- Molecular Weight:216.21
Yield:63228-62-6 96%
Reaction Conditions:
Stage #1: 3-nitro-aniline;Methanesulfonic anhydridewith triethylamine in dichloromethane at 20;
Stage #2: with sodium hydroxide in methanol;water at 20;
References:
Greenfield, Alexander;Grosanu, Cristina [Tetrahedron Letters,2008,vol. 49,# 44,p. 6300 - 6303] Location in patent:body text
