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ChemicalBook CAS DataBase List N-Acetyl-4-piperidone

N-Acetyl-4-piperidone synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 99 percent / dimethylaminopyridine; triethylamine / CH2Cl2 / 1 h / 0 °C / under nitrogen
2: 70 percent / HCl / methanol / 19 h / 20 °C

References:

Kobashi, Seiichi;Kubo, Hajime;Yamauchi, Takayasu;Higashiyama, Kimio [Biological and Pharmaceutical Bulletin,2002,vol. 25,# 8,p. 1030 - 1034]

176910-35-3 Synthesis
1,4-Dioxa-8-azaspiro[4.5]decane,  8-acetyl-  (9CI)

176910-35-3
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