P-CRESOL-D3 (METHYL-D3) synthesis
- Product Name:P-CRESOL-D3 (METHYL-D3)
- CAS Number:108561-00-8
- Molecular formula:C7H5D3O
- Molecular Weight:111.16
767-00-0
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108561-00-8
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$275.00/50mg
Yield:108561-00-8 90%
Reaction Conditions:
with palladium on activated charcoal;deuterium in hexane;water-d2;ethyl acetate at 100; under 15001.5 Torr; for 24 h;Solvent;Pressure;Reagent/catalyst;Temperature;
Steps:
13 Example 13In this Example, an aromatic deuterated methyl compound was prepared by the following preparation method,The reaction is as follows:
4-Cyanophenol (1 g) and palladium on carbon (0.1 g) were mixed in n-hexane: ethyl acetate:Deuterium water (10 mL: 1 mL: 1 mL), 2 MPa of deuterium gas,100 degrees stirring for 24 hours, after the reaction was filtered to give 4-deuteromethylphenol,Yield 90%, deuterium rate 98%.
References:
CN107353176,2017,A Location in patent:Paragraph 0079; 0080; 0081; 0082; 0083
14202-49-4
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108561-00-8
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104-93-8
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108561-00-8
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106-44-5
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108561-00-8
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1124-18-1
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21175-64-4
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25026-32-8
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108561-00-8
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70837-27-3
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