(R)-1-(4-CHLOROPHENYL)-1-PROPANOL synthesis
- Product Name:(R)-1-(4-CHLOROPHENYL)-1-PROPANOL
- CAS Number:110611-21-7
- Molecular formula:C9H11ClO
- Molecular Weight:170.64
Yield:110611-21-7 100%
Reaction Conditions:
Stage #1: diethylzincwith (Ra)-3,3'-bis(diphenylphosphinoyl)-BINOL in tetrahydrofuran;toluene at -78; for 0.5 h;
Stage #2: 4-chlorobenzaldehyde in tetrahydrofuran;toluene at -20; for 24 h;
References:
Hatano, Manabu;Miyamoto, Takashi;Ishihara, Kazuaki [Advanced Synthesis and Catalysis,2005,vol. 347,# 11-13,p. 1561 - 1568]
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