Shikimic acid synthesis
- Product Name:Shikimic acid
- CAS Number:138-59-0
- Molecular formula:C7H10O5
- Molecular Weight:174.15
88400-31-1
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138-59-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: imidazole / dimethylformamide / 1.75 h
2: 1.) H2O, AcOH; 2.) N,N-dimethylolpyridine / 1.) methanol, toluene, r.t., 1 h; 2) ether, 1 h
3: 80 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.5 h / 5 °C
4: 90 percent / aq.NaOH / methanol / 2.5 h / 5 - 25 °C
References:
Zamir, Lolita O.;Luthe, Corinne [Canadian Journal of Chemistry,1984,vol. 62,p. 1169 - 1175]
40983-58-2
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138-59-0
648 suppliers
$5.00/250mg
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91758-39-3
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138-59-0
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![1,3-Benzodioxole-5-carboxylic acid, 7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3a,6,7,7a-tetrahydro-2-methoxy-2-methyl-, methyl ester](/CAS/20210305/GIF/88400-32-2.gif)
88400-32-2
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138-59-0
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![1-Cyclohexene-1-carboxylic acid, 4-(acetyloxy)-5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-hydroxy-, methyl ester, [3S-(3α,4β,5α)]- (9CI)](/CAS/20210305/GIF/88424-81-1.gif)
88424-81-1
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138-59-0
648 suppliers
$5.00/250mg