ChemicalBook--->CAS DataBase List--->824-94-2

824-94-2

824-94-2 Structure

824-94-2 Structure
IdentificationMore
[Name]

4-Methoxybenzylchloride
[CAS]

824-94-2
[Synonyms]

1-CHLOROMETHYL-4-METHOXYBENZENE
4-(CHLOROMETHYL)ANISOL
4-(CHLOROMETHYL)ANISOLE
4-METHOXYBENZYL CHLORIDE
AKOS BBS-00003861
ANISYL CHLORIDE
METHOXYBENZYLCHLORIDE(P-)
P-METHOXYBENZYL CHLORIDE
alpha-Chloro-4-methoxytoluene
Anisole, p-(chloromethyl)-
Benzene, 1-(chloromethyl)-4-methoxy-
p-(Chloromethyl)anisole
p-Anisyl chloride
P-methoxyl benzylchloride
4-Methoxybenzylchloride99%
4-Methoxybenzylchloride 99%
4-Methoxybenzene methyl chloride
α-Chloro-4-methoxytoluene
4-Methoxybenzylchloride, stabilized, 98%
4-METHOXYBENZYL CHLORIDE (STABILIZED WITH CALCIUM CARBONATE)
[EINECS(EC#)]

212-540-6
[Molecular Formula]

C8H9ClO
[MDL Number]

MFCD00000915
[Molecular Weight]

156.61
[MOL File]

824-94-2.mol
Chemical PropertiesBack Directory
[Appearance]

Colorless liquid
[Melting point ]

−1 °C(lit.)
[Boiling point ]

117-118 °C14 mm Hg(lit.)
[density ]

1.155 g/mL at 25 °C(lit.)
[refractive index ]

n20/D 1.548(lit.)
[Fp ]

229 °F
[storage temp. ]

2-8°C
[solubility ]

Chloroform (Slightly), Ethyl Acetate (Slightly)
[form ]

Liquid
[color ]

Clear colorless to pale yellow
[Water Solubility ]

slowly decomposes
[Stability:]

Moisture Sensitive
[InChIKey]

MOHYOXXOKFQHDC-UHFFFAOYSA-N
[CAS DataBase Reference]

824-94-2(CAS DataBase Reference)
[NIST Chemistry Reference]

«alpha»-Chloro-4-methoxytoluene(824-94-2)
[Storage Precautions]

Store under inert gas
Safety DataBack Directory
[Hazard Codes ]

C
[Risk Statements ]

R34:Causes burns.
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S27:Take off immediately all contaminated clothing .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
[RIDADR ]

UN 3265 8/PG 3
[WGK Germany ]

3
[F ]

10-19-21
[Autoignition Temperature]

109℃
[Hazard Note ]

Corrosive
[TSCA ]

No
[HazardClass ]

8
[PackingGroup ]

III
[HS Code ]

29093090
Raw materials And Preparation ProductsBack Directory
[Preparation Products]

4-Methoxybenzyl cyanide-->1-(4-METHOXYBENZYL)PIPERAZINE-->1,6:2,3-Dianhydro-β-D-mannopyranose-->H-BETA,BETA-DIMETHYL-L-CYS(PMEOBZL)-OH-->4-METHOXYBENZYLMAGNESIUM CHLORIDE-->4(3H)-Pyrimidinone, 5-bromo-6-(difluoromethyl)-3-[(4-methoxyphenyl)methyl]--->1-(4-METHOXYBENZYL)-1H-INDOLE-2,3-DIONE-->Methyl 1-[(4-methoxyphenyl)methyl]-1H-indazole-3-carboxylate-->2-Propenoic acid, (4-methoxyphenyl)methyl ester-->3-bromo-6-((4-methoxybenzyl)oxy)benzaldehyde-->Carbamimidothioicacid, (4-methoxyphenyl)methyl ester, hydrochloride (1:1)-->2-Pyrimidinamine, 5-bromo-N,N-bis[(4-methoxyphenyl)methyl]--->Benzaldehyde, 2-[(4-methoxyphenyl)methoxy]-
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

1-Chloromethyl-4-methoxybenzene(824-94-2).msds
Hazard InformationBack Directory
[Chemical Properties]

Colorless liquid
[Uses]

O/N protecting group reagent which can be mildly oxidatively cleaved, e.g., with ceric ammonium nitrate.
[Synthesis Reference(s)]

Journal of Medicinal Chemistry, 20, p. 190, 1977 DOI: 10.1021/jm00212a002
The Journal of Organic Chemistry, 53, p. 3634, 1988 DOI: 10.1021/jo00250a048
[General Description]

4-Methoxybenzyl chloride undergoes mild oxidative claevage with ceric ammonium nitrate.
[Purification Methods]

Purify 4-anisyl chloride by fractional distillation under vacuum, and the middle fraction is redistilled at 10-6 mm at room temperature by intermittent cooling of the receiver in liquid N2, and the middle fraction is collected. [Mohammed & Kosower J Am Chem Soc 93 2709 1971, Beilstein 6 IV 2137.]
Spectrum DetailBack Directory
[Spectrum Detail]

4-Methoxybenzylchloride(824-94-2)1HNMR
4-Methoxybenzylchloride(824-94-2)IR1
4-Methoxybenzylchloride(824-94-2)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

4-Methoxybenzylchloride, stabilized, 98%(824-94-2)
[Sigma Aldrich]

824-94-2(sigmaaldrich)
[TCI AMERICA]

4-Methoxybenzyl Chloride  (stabilized with Amylene),>97.0%(T)(824-94-2)
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