4-Amino-N-methylbenzamide
|
|
|
- CAS-Nr.
- 6274-22-2
- Englisch Name:
- 4-Amino-N-methylbenzamide
- Synonyma:
- 4-(Methylc;4-Amino-N-methylbenz;4-Amino-N-methylbenzamide;4-Aminobenzoylmethylamide;4-(Methylcarbamoyl)aniline;Benzamide, 4-amino-N-methyl-;4-Amino-N-methylbenzamide >4-Amino-N-methylbenzamide 98%;4-Amino-N-methylbenzamide;4-Aminobenzoic acid methyl amide
- CBNumber:
- CB21054022
- Summenformel:
- C8H10N2O
- Molgewicht:
- 150.18
- MOL-Datei:
- 6274-22-2.mol
|
4-Amino-N-methylbenzamide Eigenschaften
- Schmelzpunkt:
- 181 °C
- Siedepunkt:
- 364.1±25.0 °C(Predicted)
- Dichte
- 1.137
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- Löslichkeit
- soluble in Methanol
- Aggregatzustand
- powder to crystal
- pka
- 15.84±0.46(Predicted)
- Farbe
- White to Light yellow to Light orange
- CAS Datenbank
- 6274-22-2(CAS DataBase Reference)
4-Amino-N-methylbenzamide Chemische Eigenschaften,Einsatz,Produktion Methoden
Synthese
Ammonium chloride (29.6 g, 55.4 mmol) in water (200 mL) and methanol (200 mL) was added to a solution of N-methyl-4-nitro-benzamide (10 g, 55.4 mmol) in THF (160 mL). Zinc powder (29 g, 44.4 mmol) was added portion wise and the mixture stirred for 15 minutes. The reaction mixture was filtered over celite, the filtrate was then concentrated and extracted with ethyl acetate. The organics were washed with brine solution, dried over Na2SO4 and concentrated to afford 7.2 g (86percent) of 4-Amino-N-methylbenzamide. 1H NMR: (DMSO-d6): δ 7.9 (s, 1H), 7.6 (d, 2H), 6.5 (d, 2H), 5.6 (s, 2H), 2.7 (s, 3H).
4-Amino-N-methylbenzamide Upstream-Materialien And Downstream Produkte
Upstream-Materialien
Downstream Produkte
4-Amino-N-methylbenzamide Anbieter Lieferant Produzent Hersteller Vertrieb Händler.
Global( 163)Lieferanten
6274-22-2()Verwandte Suche:
- Benzamide, 4-amino-N-methyl- (9CI)
- 4-Amino-N-methylbenzamide
- 4-AMINO-N-METHYLBENZAMIDE,98.0+%(GC)(T)
- 4-Aminobenzoylmethylamide
- 4-Amino-N-methylbenzamide
- 4-Amino-N-methylbenz
- 4-amino-N-methylbenzamide(SALTDATA: FREE)
- 4-(Methylcarbamoyl)aniline
- 4-(Methylc
- 4-Amino-N-methylbenzamide 98%
- 4-Amino-N-methylbenzamide >
- 4-(Methylcarbamyl)aniline, 98%, for synthesis
- Benzamide, 4-amino-N-methyl-
- 4-Amino-N-methylbenzamide ISO 9001：2015 REACH
- 4-Aminobenzoic acid methyl amide
- 6274-22-2
- AMIDE
- AMINEPRIMARY
- 6274-22-2
